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After ward a remedy away from 4-bromobenzyl bromide (205 mg, step 1.2 mmol) inside the N,N-dimethylformamide (4 mL) try added dropwise. After quenching with liquid, the new reaction mix is poured on the CH2Cl2 (100 mL); the fresh organic coating is wash having drinking water (50 mL) 3 x after which dehydrated over Na2SO4. After deleting the new solvent lower than smaller stress, the fresh deposit is refined by thumb chromatography for the silica solution in order to spend the money for target tool BCZ–Become. To a simple solution from dos-iodoaniline (dos.2 g, ten.0 mmol) inside the triethylamine (31.0 mL), PdCl2(PPh2)dos (70.1 mg, 0.1 mmol), CuI (58.0 mg, 0.3 mmol), and phenylacetylene (step one.2 g, several.0 mmol) were successively additional from the room-temperature under N2.

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